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    去氢甲基睾丸素的合成工艺研究

    Synthesis of methandrostenolone

      摘要
    • 摘要: 目的:研究蛋白同化激素去氢甲基睾丸素的合成工艺。方法:以去氢表雄酮醋酸酯为原料,经格氏反应,水解,沃氏氧化,DDQ脱氢等四步反应制得。结果:该合成路线不仅收率高,产品纯,而且无需过柱分离。结论:该工艺路线适合工业化生产。

       

      Abstract: OBJECTIVE:A simple procedure of four steps for the synthesis of methandrostenolone is studied.METHODS:With dehydroepiandrosterone 3 acetate as the raw material,the reactions included grignard reaction,hydrolysis,oppenauer oxidation and dehydrogen by DDQ(

       

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