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    从邻苯二甲酰亚胺合成依托酸酐

    Synthesis of Isatoic Anhydride from Phthalimide

      摘要
    • 摘要: 目的合成标题化合物,并进行工艺改进。方法以邻苯二甲酰亚胺为原料经次氯酸钠氧化合成目标化合物。结果收率达90%以上,产物经红外和核磁共振谱确证。结论改进的路线原子经济、环境友好,易操作。

       

      Abstract: OBJECTIVE To synthesize the title compound and improve the process.METHODS The title compound was synthesized from phthalimide by oxidation with sodium hypochlorite.RESULTS The yield was up to 90%,the title compound was characterized by IR and 1HNMR.CONCL

       

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