Synthesis of N,N'-bis(1-hydroxymethyl-2,3-dihydroxypropxyl)-2,3,5,6-Tetraiodo-terephthalamide

ZHANG Lai-guo; LUO Shi-neng; XIE Min-hao; LIU Xiao-ya

ZHANG Lai-guo, LUO Shi-neng, XIE Min-hao, LIU Xiao-ya. Synthesis of N,N'-bis(1-hydroxymethyl-2,3-dihydroxypropxyl)-2,3,5,6-Tetraiodo-terephthalamide[J]. Chinese Journal of Modern Applied Pharmacy, 2007, (2): 126-127.

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ZHANG Lai-guo, LUO Shi-neng, XIE Min-hao, LIU Xiao-ya. Synthesis of N,N'-bis(1-hydroxymethyl-2,3-dihydroxypropxyl)-2,3,5,6-Tetraiodo-terephthalamide[J]. Chinese Journal of Modern Applied Pharmacy, 2007, (2): 126-127.

Citation:

ZHANG Lai-guo, LUO Shi-neng, XIE Min-hao, LIU Xiao-ya. Synthesis of N,N'-bis(1-hydroxymethyl-2,3-dihydroxypropxyl)-2,3,5,6-Tetraiodo-terephthalamide[J]. Chinese Journal of Modern Applied Pharmacy, 2007, (2): 126-127.

Synthesis of N,N'-bis(1-hydroxymethyl-2,3-dihydroxypropxyl)-2,3,5,6-Tetraiodo-terephthalamide

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OBJECTIVE To design and synthesize the title compound.METHODS The title compound was synthesized from 2-butene-1,4-diol,via esterification,epoxidation,amination,then amidation with tetraiodoterebenzoyl chloride. RESULTS The structure was identified by MS,

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Synthesis of N,N'-bis(1-hydroxymethyl-2,3-dihydroxypropxyl)-2,3,5,6-Tetraiodo-terephthalamide

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