Investigation of preparation of 2-Methyl-5-Mercapto-1 ,3,4-Thiadiazole with uniform design

Wang Xu(Wang X); Li Jingfen(Li JF); Zhou Shujing(Zhou SJ) et al

Wang Xu(Wang X), Li Jingfen(Li JF), Zhou Shujing(Zhou SJ) et al, . Investigation of preparation of 2-Methyl-5-Mercapto-1 ,3,4-Thiadiazole with uniform design[J]. Chinese Journal of Modern Applied Pharmacy, 1998, (2): 31-32.

Citation:

Wang Xu(Wang X), Li Jingfen(Li JF), Zhou Shujing(Zhou SJ) et al, . Investigation of preparation of 2-Methyl-5-Mercapto-1 ,3,4-Thiadiazole with uniform design[J]. Chinese Journal of Modern Applied Pharmacy, 1998, (2): 31-32.

Citation:

Wang Xu(Wang X), Li Jingfen(Li JF), Zhou Shujing(Zhou SJ) et al, . Investigation of preparation of 2-Methyl-5-Mercapto-1 ,3,4-Thiadiazole with uniform design[J]. Chinese Journal of Modern Applied Pharmacy, 1998, (2): 31-32.

Investigation of preparation of 2-Methyl-5-Mercapto-1 ,3,4-Thiadiazole with uniform design

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The uniform design was applied to technological study of the title compound, starting from ethyl acetate and diamine hydrate,followed by reaction with carbon disulfide,the title compound was synthesized in one step.The overall yield amounts to 75.5% .

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Investigation of preparation of 2-Methyl-5-Mercapto-1 ,3,4-Thiadiazole with uniform design

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