| 摘要: |
| 目的 建立妇乐冲剂中非法成分土大黄苷的定性检测方法。方法 采用薄层色谱法、液质联用技术对怀疑有非法成分土大黄苷的妇乐冲剂进行分离分析，并采用高效液相色谱-二极管阵列检测法对其进行定性鉴别。结果 在妇乐冲剂中检测出非法成分土大黄苷。结论 该方法专属性强、灵敏度高、操作简便，可作为检测非法成分土大黄苷的有效方法。 |
| 关键词: 薄层色谱法 液质联用 妇乐冲剂 土大黄苷 非法 高效液相色谱-二极管阵列检测法 |
| DOI： |
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| Determination of Rhaponiticin Illegally Added in Fule Granule |
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JIANG Yonghai
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Shaoxing Food and Drug Control, Shaoxing 312071, China
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| Abstract: |
| OBJECTIVE To establish a method for qualitative determination of illegal composition of rhaponiticin in Fule granules. METHODS TLC and LC-MS were employed to isolate and analyze the extract from Fule granule suspected of illegal rhaponiticin and rhaponiticin was identified by HPLC-DAD. RESULTS The Fule granule was detected to contain illegal composition of rhaponiticin. CONCLUSION The established method is specific, sensitive, convenient, and can be used efficiently for control and surveillance of illegal composition of rhaponiticin. |
| Key words: TLC LC-MS Fule granule rhaponiticin illegal HPLC-DAD |
